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一、用途及适用范围
SYD-261-1石油产品闭口闪点试验器是按照中华人民共和国国家标准GB/T 261-2008《闪点的测定 宾斯基-马丁闭口杯法》所规定的要求设计制造的,适用于按GB/T 261-2008标准所规定的方法,测定闪点高于40℃的石油产品试样的闭口杯法闪点。
二、主要技术规格及参数
1、工作电源: AC220V±10%, 50Hz。
2、加热装置: ⑴ 炉体为碳化硅材料,功率为600W电热丝。
⑵ 加热功率从(0~600)W可调。
3、试样升温速率: (1~12)℃/分,手动控制。
4、电动搅拌装置: ⑴ 搅拌电机:45TYZ型恒速马达。
⑵ 传动方式:软轴联结。
⑶ 搅拌叶片规格:8㎜×40㎜。
5、搅拌速度: 符合GB/T 261-2008标准要求。
⑴ (90~120)转/分,适用于试验步骤A。
⑵ (250±10)转/分,适用于试验步骤B。
6、标准油杯: 符合GB/T 261-2008标准要求。
⑴ 内径:50.7㎜~50.8㎜。
⑵ 深度:55.7㎜~56.0㎜。
⑶ 试油容量刻线深度:33.9㎜~34.3㎜。
⑷ 试油容量:约70毫升。
7、引火装置: ⑴ 引火源:煤气(或其它民用可燃气,下同)。
⑵ 引火器孔径:0.8㎜。
8、温度计: 棒式水银温度计,符合GB/T 261-2008标准要求。
⑴ 温度范围 (-5~110)℃,分度0.5℃。
⑵ 温度范围 (20~150)℃,分度1.0℃。
⑶ 温度范围 (90~370)℃,分度2℃。
9、环境温度: ≤35℃。
10、相对湿度: ≤85%。
11、整机功耗: 不大于650W。
三、主要结构及电气原理图
(一)主要结构
本仪器主要结构见图1所示。
⑴油杯 ⑵乳胶管 ⑶进气调节阀 ⑷搅拌电机 ⑸传动软轴 ⑹引火器 ⑺温度计 ⑻弹簧旋钮 ⑼电炉 ⑽油杯座 ⑾控制面板
1、油杯: 用于盛放待测的试样。
2、乳胶管: 用于连接进气调节阀和引火器。
3、进气调节阀: 供气气源从该阀进气口接入,用于调节点火器供气的大小。
4、搅拌电机: 用于搅拌油杯中的试样。
5、传动软轴: 连接搅拌电机和搅拌叶片。
6、引火器: 用于调节火焰的大小和关闭、打开煤气。
7、温度计: 符合GB/T 261-2008标准要求。
8、弹簧旋钮: 用于手动点火。
9、电炉: 用于加热油杯中的试样。
10、油杯座: 用于放置油杯。
11、控制面板: 见下节(控制面板)。
(二)控制面板
控制面板见图2所示。
1、步骤A按钮: 在搅拌选择开关打开的情况下,按动此按钮指示灯亮,搅拌电机的转速是90~120转/分,适用于按步骤A的要求试验。
2、搅拌选择开关: 搅拌电机工作控制开关。按下此开关指示灯亮,搅拌电机接通工作电源(注:本仪器搅拌电机默认的搅拌速度是90~120转/分,为试验步骤A的搅拌速度)。
3、步骤B按钮: 在搅拌选择开关打开的情况下,按动此按钮指示灯亮,搅拌电机的转速是250±10转/分,适用于按步骤B的要求试验。
4、电源开关: 打开此开关,指示灯亮,仪器接通工作电源。
5、电压表: 指示电炉的加热电压值。
6、加热调节: 加热功率调节旋钮,加热电炉的加热电压在电压表上指示。
(二)电气原理
仪器电路主要由加热、加热调节、搅拌系统组成。
电源开关一打开,加热电炉即开始加热。双向可控硅FS组成交流调压电路,调节“加热调节旋钮”,可调节加热电炉的功率,其工作电压在电压表上显示。
搅拌装置由两种转速可供选择,90~120转/分,适用于步骤A试验方式;250±10转/分,适用于步骤B试验方式。搅拌装置是否工作则由搅拌开关控制。
四、仪器的使用
1、使用本仪器前应仔细阅读使用说明书。
2、仔细阅读中华人民共和国标准GB/T 261-2008《闪点的测定 宾斯基-马丁闭口杯法》,了解并熟悉标准所阐述的试验方法、试验步骤和试验要求。
3、按GB/T261-2008标准所规定的要求,仪器放置在光线较暗且避风的地方以便观察闪火,准备好试验用的各种试验器具、材料等。
4、检查本仪器的工作状态,使其符合说明书所规定的工作环境和工作条件。
5、检查本仪器的外壳,必须处于良好的接地状态。
6、油杯盛放定量的试样后按图1所示置于加热炉上,并将杯盖、搅拌装置、温度计等按要求安放到位。
7、根据试验要求选择步骤A或者步骤B,将搅拌速度选择并确定在所需的试验状态。
8、按GB/T261-2008标准所规定的升温要求随时注意控温调节(即调节“加热调节旋钮”控制电炉加热功率,加热电压由电压表检测并显示)。
9、当试样油温达到预期闪点前,按标准所规定的温度点,通放煤气,点燃引火器,调整火焰形状至标准要求。
10、调节弹簧旋钮使滑板转动,露出油杯盖孔口,同时,引火器即自动向下摆动,伸向油杯盖点火孔内进行点火试验。
11、继续按GB/T261-2008标准所规定的要求与步骤试验,直至取得试验结果。
注意:仪器使用步骤和要求,应严格按照GB/T 261-2008标准所规定的要求进行。
五、注意事项
1、 电源线必须有良好的接地端,确保用电的安全。
2、 仪器使用完毕必须关闭外接可燃气源的阀门。
3、仪器不用时,关闭电源开关、加热开关及搅拌开关,置于通风干燥处。
4、备用油杯不加热时,可安放在油杯座内,谨防翻倒叩伤。
5、本仪器适用于闭口闪点温度为280℃以下的油品试验。
6、仪器电路发生故障时,须请专业人员进行检修。
警告:仪器若出现故障应及时切断电源,待仪器冷却至室温后请专业人员检修并排除故障后方可继续使用,防止发生意外!
六、仪器成套及技术文件
1、仪器成套
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mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>支 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>1 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">GB/T261-2008 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; 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mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>7 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">电源线(250V normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>根 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>1 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly"> normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>8 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">保险丝 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>只 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>2 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly"> normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>9 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">温度计适配器 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>套 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>1 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly"> normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-left: 11.0pt; ms, o-element-top: 13.25pt; mso-height-rule: exactly; mso-element-anchor-horizonta: margin" align=center>10 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">温度计衬带 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">(剪适量卷在温度计下端,使温度计正好插在温度计适配器内) normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>片 normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly" align=center>5 normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; mso-element: frame; mso-element-frame-hspace: 9.0pt; mso-element-wrap: around; mso-element-anchor-vertical: paragraph; mso-element-anchor-horizontal: margin; mso-element-left: 11.0pt; mso-element-top: 13.25pt; mso-height-rule: exactly">normalTable style="BORDER-RIGHT: medium none; BORDER-TOP: medium none; MARGIN-LEFT: 6.75pt; BORDER-LEFT: medium none; MARGIN-RIGHT: 6.75pt; BORDER-BOTTOM: medium none; BORDER-COLLAPSE: collapse; mso-border-alt: solid windowtext .5pt; mso-table-lspace: 9.0pt; mso-table-rspace: 9.0pt; mso-table-anchor-vertical: paragraph; mso-table-anchor-horizontal: margin; mso-table-left: 10.95pt; mso-table-top: 13.25pt; mso-padding-alt: 0cm 5.4pt 0cm 5.4pt; mso-border-insideh: .5pt solid windowtext; mso-border-insidev: .5pt solid windowtext" cellSpacing=0 cellPadding=0 align=left border=1>
2、技术文件
⑴ 使用说明书 1份
⑵ 合格证 1份
⑶ 产品保修卡 1份
七、常见故障及排除方法
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>序号 |
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>常见故障 |
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>原 因 |
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>排除方法 |
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>1 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">电源指示灯不亮 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">停电 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查外电源 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">保险丝坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换保险丝 | ||
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">电源开关坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换开关 | ||
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>2 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly">电压表不指示 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">保险丝坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换保险丝 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">电压表坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换电压表 | ||
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>3 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly">电炉不加热 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">电炉电热丝断 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换电热丝 |
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>4 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly">加热调节不起作用 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">双向可控硅FS坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换可控硅FS |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">调节电位器坏 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并更换调节电位器 | ||
normal style="LINE-HEIGHT: 18pt; TEXT-ALIGN: center; mso-line-height-rule: exactly; tab-stops: 27.0pt" align=center>5 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly">搅拌不转 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">搅拌开关未打开 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">打开搅拌控制开关 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">电机连线脱落 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查并接好电机连线 | ||
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">控制板故障 |
normal style="LINE-HEIGHT: 18pt; mso-line-height-rule: exactly; tab-stops: 27.0pt">检查搅拌控制板,排除故障 |
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